Synthesis Of An Iron ( IIi ) -oxalate Complex - 1423 Words

EXPERIMENT 4A: Synthesis of an Iron(III)-Oxalate Complex: To begin, a filtering crucible was washed, labeled, and dried in an oven for one hour. While the experiment was performed, the filtering crucible was set-aside in a desiccator to cool and stay dry. After this was done, a mass of about 1.2 g ( ±0.2 g) of iron(II) ammonium sulfate hydrated salt (Fe(NH4)2(SO4)2 ∙ 6H2O) was measured and recorded. It was then placed in a 50-mL beaker with 3 mL of deionized water and 1-3 drops of 6M sulfuric acid. The beaker was then swirled until all of the salt particles dissolved. Then, about 6 mL of 1 M oxalic acid was added to the solution in the 50-mL beaker. At this point, the pH was checked to ensure that solution was acidic. If it wasn’t acidic, then an addition of 6 M sulfuric acid may have been needed. This solution was then gently boiled, with boiling chips, for about five minutes to break down the precipitate. While the solution boiled, it was essential to swirl the solut ion. Once the solution had cooled down, the supernatant was decanted and put in a waste beaker, and the precipitate was washed with clean, hot deionized water. This precipitate was rinsed three times. The supernatant and wash solution wastes were then thrown away in waste containers. Then, 3.5 mL of 1.7 M potassium oxalate solution were added to the beaker with the rinsed precipitate. This solution was warmed to about 40â„Æ' and it was constantly stirred. The solution was then removed from the Bunsen burner, andShow MoreRelatedSynthesis and Component Analysis of an Iron (Iii) Oxalate Complex7868 Words   |  32 PagesExperiments 4A-C: Synthesis and Component Analysis of an Iron (III) Oxalate Complex My Name TA, Section B## Work Performed on 10/23, 10/30, 11/4, 200# Report due Tuesday, November ##, 200# 1. Abstract This experiment initially involved the synthesis of an iron (III) oxalate complex with the general formula Kw[Fex(C2O4)y] ·zH2O. The variables x, y, and z were determined through the duration of the entire experiment. From 1.2000g of Fe(NH4)2(SO4)2 were synthesized 1.1###g of K3[FeIII(C2O4)3] ·3H2ORead MoreSynthesis and Component Analysis of an Iron (Iii) Oxalate Complex7868 Words   |  32 PagesExperiments 4A-C: Synthesis and Component Analysis of an Iron (III) Oxalate Complex My Name TA, Section B## Work Performed on 10/23, 10/30, 11/4, 200# Report due Tuesday, November ##, 200# 1. Abstract This experiment initially involved the synthesis of an iron (III) oxalate complex with the general formula Kw[Fex(C2O4)y] ·zH2O. The variables x, y, and z were determined through the duration of the entire experiment. From 1.2000g of Fe(NH4)2(SO4)2 were synthesized 1.1###g of K3[FeIII(C2O4)3] ·3H2ORead MoreOxalate Lab Essay609 Words   |  3 PagesNovember 8th, 2010 Synthesis and Analysis of Iron(III) Oxalate Complex Discussion This experiment initially involved the synthesis of an iron (III) oxalate complex with the general formula Kw[Fex(C2O4)y] zH2O. The variables x, y, and z were determined through the duration of the entire experiment. Part 1 involves the synthesis of an iron (III) oxalate complex. The iron is first presented in its Fe2+ form, so it must first be oxidized to Fe3+ before the oxalate ion will readily bindRead MoreIons in Our Daily Life2554 Words   |  11 Pagesincluding the ion channels gramicidin and amphotericin (a fungicide). Inorganic dissolved ions are a component of total dissolved solids, an indicator of water quality in the world. Chemistry Notation Denoting the charged state Equivalent notations for an iron atom (Fe) that lost two electrons. When writing the chemical formula for an ion, its net charge is written in superscript immediately after the chemical structure for the molecule/atom. The net charge is written with the magnitude before the sign;Read MoreThe Extraction of Pectin from Orange Peels13647 Words   |  55 Pagesproduced by the use of 0.17% HCL as extracting agent and ethanol volumetric ratio of 0.67 for precipitation are recommended. TABLE OF CONTENTS Title Page - - - - - - - - i Certification - - - - - - - ii Dedication - - - - - - - iii Acknowledgement - - - - - - iv Abstract - - - - - - - v Table of Contents - - - -- - - vi List of Figures - - - - - - ix List of Tables - - - - - - - x CHAPTER ONE 1. Introduction - - - - - - 1-3 1.2 Objectives